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小檗碱可溶性粒剂的制备及室内杂草防治

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田亚, 张伟, 董艺珂, 等. 小檗碱可溶性粒剂的制备及室内杂草防治[J]. 植物医学, 2021, (6): 50-57. doi: 10.13718/j.cnki.zwys.2021.06.010
引用本文: 田亚, 张伟, 董艺珂, 等. 小檗碱可溶性粒剂的制备及室内杂草防治[J]. 植物医学, 2021, (6): 50-57. doi: 10.13718/j.cnki.zwys.2021.06.010
shu
TIAN Ya, ZHANG Wei, DONG Yike, et al. Preparation of Berberine Soluble Granules and Its Effiency of Weed Control[J]. PLANT HEALTH AND MEDICINE, 2021, (6): 50-57. doi: 10.13718/j.cnki.zwys.2021.06.010
Citation: TIAN Ya, ZHANG Wei, DONG Yike, et al. Preparation of Berberine Soluble Granules and Its Effiency of Weed Control[J]. PLANT HEALTH AND MEDICINE, 2021, (6): 50-57. doi: 10.13718/j.cnki.zwys.2021.06.010
shu

小檗碱可溶性粒剂的制备及室内杂草防治

  • 1. 西南大学 植物保护学院, 重庆 400715;

  • 2. 四川省农业农村厅植物保护站, 成都 610041;

  • 3. 西藏自治区农牧科学院蔬菜研究所, 拉萨 850000;

  • 4. 山东滨农科技有限公司, 山东 滨州 256603

详细信息

Preparation of Berberine Soluble Granules and Its Effiency of Weed Control

  • 1. School of Plant Protection, Southwest University, Chongqing 400715, China;

  • 2. Plant Protection Station of Department of Agriculture and Rural Affairs of Sichuan Province, Chengdu 610041, China;

  • 3. Vegetables Institute of Xizang Academy of Agriculture and Animal Husbandry Sciences, Lhasa 850000, China;

  • 4. Shandong Binnong Technology Co., Ltd, Binzhou Shandong 256603, China

  • 摘要: 小檗碱（Berberine）是一种从中药黄连中分离的异喹啉生物碱，具有杀菌、杀虫和除草活性.本研究采用挤压造粒法制备小檗碱可溶性粒剂，通过单因素试验对载体、分散剂、润湿剂、结剂、崩解剂等主要助剂的种类和用量进行筛选，结果发现，30％小檗碱可溶性粒剂研制的最佳配方为30%小檗碱、10％木质素磺酸钠、7％聚羧酸sp-2845w、2％聚乙烯醇盐、7％氯化钠和44％无水硫酸钠.进一步通过室内土壤处理法对狗尾草Setaria viridis L.进行防治试验，结果表明30%硫酸小檗碱可溶性粒剂的防治效果显著性优于30%盐酸小檗碱可溶性粒剂，其在弱碱性条件下（pH值为9），3，7，14 d的防效分别为74.24%，66.01%和68.17%，而且显著性抑制狗尾草的生长.
    Abstract: Berberine,an isoquinoline alkaloid isolated from the traditional Chinese medical plant Coptis chinensis,exhibits bactericidal,insecticidal and herbicidal activity. In order to provide theoretical support and technical guidance for the production of berberine-base pesticides,soluble granules were prepared using extrusion granulation. Through single-factor screening tests,the types and amounts of major additives (carriers,dispersants,wetting agents,binders and disintegrators) were screened and optimized. The optimized formulation of the obtained 30% berberine soluble granules was found to be 30% berberine +10% sodium ligninsulfonate +7% polycarboxylate sp-2845w +2% polyvinyl alcohol-vinylalcohol polymer +7% NaCl +44% anhydrous Na2SO4. Furthermore,the indoor soil treatment method was used to control green bristlegrass (Setaria viridis L.). The results showed that the control effect of 30% berberine sulfate soluble granule was significantly better than that of 30% berberine hydrochloride soluble granule. Under the condition of weak alkalinity (pH=9),the control effects were 74.24%,66.01% and 68.17% for 3,7 and 14 days,respectively,and significantly inhibited the growth of green bristlegrass.
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  • [1] HU H Y, LI K P, WANG X J, et al. Set9, NF-κB, and MicroRNA-21 Mediate Berberine-Induced Apoptosis of Human Multiple Myeloma Cells[J]. Acta Pharmacologica Sinica, 2013, 34(1):157-166.
    [2] JANTOVA S, CIPAK L, LETASIOVA S. Berberine Induces Apoptosis through a Mitochondrial/Caspase Pathway in Human Promonocytic U937 Cells[J]. Toxicology in Vitro, 2007, 21(1):25-31.
    [3] VIEIRA S, CASTELLI S, FALCONI M, et al. Role of 13-(Di) Phenylalkyl Berberine Derivatives in the Modulation of the Activity of Human Topoisomerase IB[J]. International Journal of Biological Macromolecules, 2015, 77:68-75.
    [4] YIN J, GAO Z, LIU D, et al. Berberine Improves Glucose Metabolism through Induction of Glycolysis[J]. American Journal of Physiology Endocrinology and Metabolism, 2008, 294(1):148-156.
    [5] IWASA K, MORIYASU M, NADER B. Fungicidal and Herbicidal Activities of Berberine Related Alkaloids[J]. Bioscience, Biotechnology, and Biochemistry, 2000, 64(9):1998-2000.
    [6] LEE C H, LEE H J, JEON J H, et al. In Vivo Antifungal Effects of Coptis japonica Root-Derived Isoquinoline Alkaloids Against Phytopathogenic Fungi[J]. Journal of Microbiology&Biotechnology, 2005, 15(6):1402-1407.
    [7] 赵立峰.小檗碱类化合物的合成及其生物活性的测定[D].贵阳:贵州大学, 2009.
    [8] 李明,曾唏,季祥彪,等.盐酸黄连素对蚜虫生物活性的研究[J].昆虫学报, 1999, 42(2):140-144.
    [9] MIYAZAWA M, FUJIOKA J, ISHIKAWA Y. Insecticidal Compounds from Phellodendron Amurense Active Against Drosophila Melanogaster[J]. Journal of the Science of Food and Agriculture, 2002, 82(8):830-833.
    [10] WU J, MA J J, LIU B, et al. Herbicidal Spectrum, Absorption and Transportation, and Physiological Effect on Bidens Pilosa of the Natural Alkaloid Berberine[J]. Journal of Agricultural and Food Chemistry, 2017, 65(30):6100-6113.
    [11] BI X D, ZHANG S L, ZHANG B, et al. Effects of Berberine on the Photosynthetic Pigments Compositions and Ultrastructure of Cyanobacterium Microcystis Aeruginosa[J]. Advanced Materials Research, 2011, 343-344:1117-1125.
    [12] 毕相东,张树林,丛方地,等.盐酸小檗碱纳米乳的抑藻性能研究[J].环境科学与技术, 2014, 37(6):21-24, 43.
    [13] 朱宗林. 50%烯啶虫胺可溶性粒剂关键技术及产业化研究[D].北京:北京化工大学, 2011.
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  • 收稿日期:  2021-07-21

小檗碱可溶性粒剂的制备及室内杂草防治

  • 收稿日期:  2021-07-21
基金项目: 

摘要: 小檗碱（Berberine）是一种从中药黄连中分离的异喹啉生物碱，具有杀菌、杀虫和除草活性.本研究采用挤压造粒法制备小檗碱可溶性粒剂，通过单因素试验对载体、分散剂、润湿剂、结剂、崩解剂等主要助剂的种类和用量进行筛选，结果发现，30％小檗碱可溶性粒剂研制的最佳配方为30%小檗碱、10％木质素磺酸钠、7％聚羧酸sp-2845w、2％聚乙烯醇盐、7％氯化钠和44％无水硫酸钠.进一步通过室内土壤处理法对狗尾草Setaria viridis L.进行防治试验，结果表明30%硫酸小檗碱可溶性粒剂的防治效果显著性优于30%盐酸小檗碱可溶性粒剂，其在弱碱性条件下（pH值为9），3，7，14 d的防效分别为74.24%，66.01%和68.17%，而且显著性抑制狗尾草的生长.

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